
濟南聚大邦成化工有限公司
聯系人:張總
電話:13583111587
網址:www.bofengdl.com
地址:濟南市天橋區新材料市場南區7-1-1
精萘廠家:提取的方法
精萘的提取可以通過多種方法進行,以下是幾種常見的精萘提取方法:
The extraction of refined naphthalene can be carried out through various methods, and the following are several common methods for extracting refined naphthalene:
煤焦油提取法 :
Coal tar extraction method:
從高溫煤焦油中分離出萘油餾分(210-230℃),經過洗滌脫酚和精餾分離輕組分,得到工業萘。
Separate naphthalene oil fraction (210-230 ℃) from high-temperature coal tar, wash and dephenolate, and separate light components by distillation to obtain industrial naphthalene.
工業萘進一步通過酸洗和蒸餾,硫含量可降至小于0.1%,再通過加氫精制工藝,硫含量可低于0.05%。
Industrial naphthalene can further reduce its sulfur content to less than 0.1% through acid washing and distillation, and then through hydrogenation refining process, its sulfur content can be reduced to less than 0.05%.
結晶法 :
Crystallization method:
利用不同純度萘的熔點差異,通過分步結晶和融化操作,高結晶點萘進入成品槽,低純度萘進入殘油罐。
By utilizing the melting point differences of different purity naphthalenes, high crystallization point naphthalenes enter the finished product tank and low purity naphthalenes enter the residual oil tank through step-by-step crystallization and melting operations.
在精制工序中,通過閃蒸進一步精制制得精萘。
In the refining process, refined naphthalene is further refined by flash evaporation.
溶劑萃取法 :
Solvent extraction method:
使用乙醇對煤焦油進行萃取,然后對萃出液減壓蒸餾,得到含萘量較高的固液混合物,經過濾抽干得到粗萘。
Ethanol is used to extract coal tar, and then the extracted liquid is subjected to vacuum distillation to obtain a solid-liquid mixture with high naphthalene content. After filtration and dehydration, crude naphthalene is obtained.
水蒸汽蒸餾法 :
Steam distillation method:
建立水蒸汽蒸餾提純粗萘的方法,所得精萘純度可達99.48%,回收率在93%以上。
Establishing a method for steam distillation purification of crude naphthalene, the purity of refined naphthalene obtained can reach 99.48%, with a recovery rate of over 93%.
分步結晶法 :
Stepwise crystallization method:
將工業萘裝入箱式結晶器中,根據萘中各餾分結晶點的差別進行分步結晶提純。
Load industrial naphthalene into a box type crystallizer and perform step-by-step crystallization purification based on the differences in crystallization points of each fraction in naphthalene.
豎管式結晶法 :
Vertical tube crystallization method:
利用豎管式結晶器進行多級結晶過程,包括結晶、發汗和熔融步驟,生產出高純度的精萘。
Using a vertical tube crystallizer for multi-stage crystallization process, including crystallization, sweating, and melting steps, high-purity refined naphthalene is produced.
反應與精餾結合法 :
Reaction and distillation combined method:
以工業萘為原料,通過過氧化氫氧化和有機酸、無機酸催化,結合精餾方法提取精萘。
Using industrial naphthalene as raw material, refined naphthalene is extracted through hydrogen peroxide oxidation, organic acid and inorganic acid catalysis, and distillation method.
以上方法中,結晶法和分步結晶法因其高純度和節能效果而被廣泛應用。選擇具體提取方法時,需要考慮原料來源、成本、環境影響及生產規模等因素。
Among the above methods, crystallization and stepwise crystallization are widely used due to their high purity and energy-saving effects. When selecting a specific extraction method, factors such as raw material sources, costs, environmental impact, and production scale need to be considered.
本文由精萘廠家為您提供,我們的網站是:http://www.bofengdl.com我們將以全心全意的熱情為您提供服務,歡迎您的訪問!
This article is provided by the refined naphthalene manufacturer. Our website is: http://www.bofengdl.com We will provide you with wholehearted enthusiasm and welcome your visit!
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